Mounting powder samples for sub-Kelvin neutron diffraction

  1. Get@NRC: Mounting powder samples for sub-Kelvin neutron diffraction (Opens in a new window)
DOIResolve DOI:
AuthorSearch for: ; Search for:
Journal titleJournal of Applied Crystallography
Pages4347; # of pages: 5
SubjectNeutron; powder sample mounting; sub-Kelvin temperatures; neutron powder diffraction
AbstractThe increasing availability of 3He-based cryostats is making it possible to add sub-Kelvin capabilities to powder diffraction instruments. However, there are many problems associated with cooling powders below 1 K, and if great care is not taken, the sample temperature may be far higher than that reported by a thermometer attached to the sample holder. This contribution describes two practical and effective strategies for mounting powder samples that yield equilibration times of at most a few tens of minutes.
Publication date
PublisherInternational Union of Crystallography
Copyright noticeThe International Union of Crystallography permits archiving of pre- and post-print; they encourage use of the publisher's version/PDF in the institutinal repository.
AffiliationNational Research Council Canada (NRC-CNRC); NRC Canadian Neutron Beam Centre
Access conditionavailable
Peer reviewedYes
NPARC number9201849
Export citationExport as RIS
Report a correctionReport a correction
Record identifier32efbe94-2b4c-4a26-9457-c06063b10dcb
Record created2009-10-02
Record modified2016-05-09
Bookmark and share
  • Share this page with Facebook (Opens in a new window)
  • Share this page with Twitter (Opens in a new window)
  • Share this page with Google+ (Opens in a new window)
  • Share this page with Delicious (Opens in a new window)