Mounting powder samples for sub-Kelvin neutron diffraction

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DOIResolve DOI: http://doi.org/10.1107/S002188980803570X
AuthorSearch for: ; Search for:
TypeArticle
Journal titleJournal of Applied Crystallography
ISSN0021-8898
Volume42
Issue1
Pages4347; # of pages: 5
SubjectNeutron; powder sample mounting; sub-Kelvin temperatures; neutron powder diffraction
AbstractThe increasing availability of 3He-based cryostats is making it possible to add sub-Kelvin capabilities to powder diffraction instruments. However, there are many problems associated with cooling powders below 1 K, and if great care is not taken, the sample temperature may be far higher than that reported by a thermometer attached to the sample holder. This contribution describes two practical and effective strategies for mounting powder samples that yield equilibration times of at most a few tens of minutes.
Publication date
PublisherInternational Union of Crystallography
Copyright noticeThe International Union of Crystallography permits archiving of pre- and post-print; they encourage use of the publisher's version/PDF in the institutinal repository.
LanguageEnglish
AffiliationNational Research Council Canada (NRC-CNRC); NRC Canadian Neutron Beam Centre
Access conditionavailable
unlimited
public
Peer reviewedYes
NPARC number9201849
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Record identifier32efbe94-2b4c-4a26-9457-c06063b10dcb
Record created2009-10-02
Record modified2016-05-09
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