Headspace single-drop microextration for the detection of organotin compounds

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DOIResolve DOI: http://doi.org/10.1016/j.talanta.2003.11.035
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TypeArticle
Journal titleTalanta
ISSN0039-9140
Volume63
IssueJune 17 3
Pages555560; # of pages: 6
SubjectLiquid–liquid extraction; Gas chromatography; Supercritical fluid extraction
AbstractThe performance of single-drop microextraction (SDME), coupled with gas chromatography/mass spectrometry, was assessed for the determination of tributyltin compounds in water and solid samples. Experimental parameters impacting the performance of SDME, such as microextraction solvent and sampling and stirring time, were investigated. Analytical results obtained by SDME were compared with those generated by conventional solid phase microextraction (SPME) and liquid–liquid extraction (LLE) for the determination of TBT in PACS-2 sediment certified reference material (CRM).
Publication date
LanguageEnglish
AffiliationNRC Institute for National Measurement Standards; National Research Council Canada
Peer reviewedNo
Identifier10294570
NRC number459
NPARC number8897410
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Record identifierbba4705f-4b34-4f19-a924-f80d09661390
Record created2009-04-22
Record modified2016-05-09
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