Performance of Cu-coated vanadium cans for in situ neutron powder diffraction experiments on hydrogen storage materials

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DOIResolve DOI: http://doi.org/10.1107/S002188981202938X
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TypeArticle
Journal titleJournal of Applied Crystallography
Volume45
Issue5
Pages902905; # of pages: 4
AbstractIn situ neutron powder diffraction (NPD) measurements of hydrogenation processes taking place at high temperatures pose difficulties related to the choice of sample can material. This article describes a simple design for a copper-coated vanadium can and its connection to the gas-handling system, tested up to 523 K. High-quality NPD patterns of TiV1.2Mn0.8 body-centred cubic alloy, as-cast and partially hydrogenated, were collected at 373 K and deuterium pressures up to 2 bar (200 kPa).
Publication date
PublisherWiley
LanguageEnglish
AffiliationNRC Canadian Neutron Beam Centre; National Research Council Canada
Peer reviewedYes
NPARC number20827871
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Record identifierf5c43965-9a75-4b1b-884d-3fefb8cb52e9
Record created2012-10-26
Record modified2016-05-09
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