TY  - JOUR
ID  - 20955687
AU  - Hanson, Margaret A.
AU  - Sutrisno, Andre
AU  - Terskikh, Victor V.
AU  - Baines, Kim M.
AU  - Huang, Yining
T1  - Solid-state (73) Ge NMR spectroscopy of simple organogermanes
JO  - Chemistry : a European Journal
PB  - Wiley
SP  - 13770
EP  - 13779
VL  - 18
IS  - 43
PY  - 2012
KW  - density functional calculations; germanium; NMR spectroscopy
N2  - Germanium-73 is an extremely challenging nucleus to examine by NMR spectroscopy due to its unfavorable NMR properties. Through the use of an ultrahigh (21.1 T) magnetic field, a systematic study of a series of simple organogermanes was carried out. In those cases for which X-ray structural data were available, correlations were drawn between the NMR parameters and structural metrics. These data were combined with DFT calculations to obtain insight into the structures of several compounds with unknown crystal structures.
M1  - 
DO  - http://dx.doi.org/10.1002/chem.201201944
U3  - Measurement Science and Standards
U3  - Science des mesures et étalons (SME-MSS)
U3  - National Research Council Canada
U3  - Conseil national de recherches Canada (CNRC-NRC)
ER  -